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3D-printed flow system for determination of lead in natural waters ArchiMer
Mattio, Elodie; Robert-peillard, Fabien; Branger, Catherine; Puzio, Kinga; Margaillan, Andre; Brach-papa, Christophe; Knoery, Joel; Boudenne, Jean-luc; Coulomb, Bruno.
The development of 3D printing in recent years opens up a vast array of possibilities in the field of flow analysis. In the present study, a new 3D-printed flow system has been developed for the selective spectrophotometric determination of lead in natural waters. This system was composed of three 3D-printed units (sample treatment, mixing coil and detection) that might have been assembled without any tubing to form a complete flow system. Lead was determined in a two-step procedure. A preconcentration of lead was first carried out on TrisKem Pb Resin located in a 3D-printed column reservoir closed by a tapped screw. This resin showed a high extraction selectivity for lead over many tested potential interfering metals. In a second step, lead was eluted by...
Tipo: Text Palavras-chave: Lead determination; 3D-printed MPFS system; Stereolithography; Natural waters.
Ano: 2017 URL: https://archimer.ifremer.fr/doc/00377/48770/49290.pdf
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3D-printed lab-on-valve for fluorescent determination of cadmium and lead in water ArchiMer
Mattio, Elodie; Robert-peillard, Fabien; Vassalo, Laurent; Branger, Catherine; Margaillan, Andre; Brach-papa, Christophe; Knoery, Joel; Boudenne, Jean-luc; Coulomb, Bruno.
In recent years, the development of 3D printing in flow analysis has allowed the creation of new systems with various applications. Up to now, 3D printing was mainly used for the manufacture of small units such as flow detection cells, preconcentration units or mixing systems. In the present study, a new 3D printed lab-on-valve system was developed to selectively quantify lead and cadmium in water. Different technologies were compared for lab-on-valve 3D printing. Printed test units have shown that stereolithography or digital light processing are satisfactory techniques for creating complex lab-on-valve units. The lab-on-valve system was composed of two columns, eight peripheral ports and a central port, and a coil integrating baffles to increase mixing...
Tipo: Text Palavras-chave: Stereolithography; Digital light processing; LOV-MSFIA; Natural waters.
Ano: 2018 URL: https://archimer.ifremer.fr/doc/00427/53874/54932.pdf
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Toward Chalcogenide Platform Infrared Sensor Dedicated to the In Situ Detection of Aromatic Hydrocarbons in Natural Waters via an Attenuated Total Reflection Spectroscopy Study ArchiMer
Baillieul, Marion; Baudet, Emeline; Michel, Karine; Moreau, Jonathan; Němec, Petr; Boukerma, Kada; Colas, Florent; Charrier, Joël; Bureau, Bruno; Rinnert, Emmanuel; Nazabal, Virginie.
he objective of this study is to demonstrate the successful functionalization of the surface of a chalcogenide infrared waveguide with the ultimate goal of developing an infrared micro-sensor device. First, a polyisobutylene coating was selected by testing its physico-chemical compatibility with a Ge-Sb-Se selenide surface. To simulate the chalcogenide platform infrared sensor, the detection of benzene, toluene, and ortho-, meta- and para-xylenes was efficaciously performed using a polyisobutylene layer spin-coated on 1 and 2.5 µm co-sputtered selenide films of Ge28Sb12Se60 composition deposited on a zinc selenide prism used for attenuated total reflection spectroscopy. The thickness of the polymer coating was optimized by attenuated total reflection...
Tipo: Text Palavras-chave: Optical infrared sensor; Chalcogenide glasses; Mid-infrared; Mono-aromatic hydrocarbons; Natural waters; BTEXs; PAHs.
Ano: 2021 URL: https://archimer.ifremer.fr/doc/00687/79947/82867.pdf
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